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  • Domain size distribution of Y-TZP nano-particles using XRD and HRTEM
    Boulc'h, Florence ...
    Yttria doped nanocrystalline zirconia powder was prepared by spray-pyrolysis technique. Powder crystallized into tetragonal form, as dense and compositionally homogeneous polycrystalline spheres. ... X-Ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) have been used inorder to characterize the mean size and the size distribution of crystallinedomains. An average size of 6 nm was calculated by Scherrer formulafrom X-Ray diffraction pattern. The domain size, determined by analysismethod developed by Hytch from HRTEM observations, ranges from 5 to 22nm with a main population around the value 12 nm. Limits and complementary nature of XRD and HRTEM methods are discussed.
    Vir: Image analysis & stereology : official journal of the International Society for Stereology. - ISSN 1580-3139 (Vol. 20, no. 3, nov. 2001, str. 157-161)
    Vrsta gradiva - članek, sestavni del
    Leto - 2001
    Jezik - angleški
    COBISS.SI-ID - 16036057

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    Digitalna knjižnica Slovenije - dLib.si

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