Central Technological Library of the University of Ljubljana (CTK)
13.
Katalitične in nekatalitične modelne reakcije v mikrovalovnih reaktorjih
Plazl, Igor ; Pipuš, Goran ; Koloini, Tine, 1940-2008
Rokopis predstavlja študij vpliva mikrovalov na reakcijsko kinetiko nekaterih katalitičnih in nekatalitičnih modelnih reakcij (hidroliza saharoze v fruktozo in glukozo, kislo-katalizirana ...esterifikacija benzojeve kisline z etanolom) v mikrovalovnih rekatorjih. Pri študiju smo uporabljali standardni laboratorijski mešalni reaktor in pretočni cevni reaktor, postavljena v prirejeno komercialno mikrovalovno pečico. Postavili smo tudi nov mikrovalovni reaktorski sistem, kjer mikrovalove dovajamo v reaktor po valovodih. Ta izvedba reaktorjev omogoča študij modelnih reakcij pri kontroliranih visokih tlakih in temperaturah. Mikrovalovno aparaturo poenostavljeno sestavljajo: generator (vir mikrovalov), sestavni deli valovodnega sklopa (transport mikrovalov) in breme (reaktor, kjer se mikrovalovna moč pretvori v toplotno energijo).
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