Production of biomaterials from cork : Liquefaction in polyhydric alcohols at moderate temperatures
Cheumani-Yona, Arnaud Maxime ...
The aim of this study was to develop polymers in a liquid solution, from renewable bio-resources, usable as intermediate materials in the preparation of plastics, adhesives or coatings. The ...liquefaction of cork with glycerol was investigated at 150 °C, 180 °C, and 200 °C under acidic (sulphuric acid) or alkaline conditions (sodium hydroxide). Cork appears as a two-component material, containing suberin and lignocelluloses. In the presence of sulphuric acid, only the liquefaction of the lignocellulosic components was achieved, leading to liquefaction yield of less than 47% at all investigated conditions. The inverse phenomenon was observed with sodium hydroxide. Suberin was almost completely liquefied, but an increase of temperature and/or sodium hydroxide content was necessary to improve the liquefaction of lignocelluloses. Addition of polyethylene glycol to glycerol to a certain extent caused the conversion of suberin under acid conditions leading to liquefaction yield up to 93%. Therefore, it was demonstrated that it is possible to use cork dust, a less valuable by-product, for the production of various basic chemicals and/or polymers with a high added value.
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