This study investigated the effect of the oak chips added at different dosages and stages of apple wine production on its oenological, antioxidant and sensory properties. In the study, medium-toasted ...or heavily-toasted oak chips (at a concentration of 3 or 6 g/L) and ethanol extracts prepared from them (at a dose of 1 or 2 mL/100 mL) were used. Basic oenological parameters (OIV), total polyphenol content (Folin-Ciocalteu method), antioxidant activity (ABTS assay), color (CIELAB) and organoleptic assessment of the wine were evaluated. Although the use of chips had no significant effect on the ethanol content and wine extract, it caused a significant change in volatile acidity. Furthermore, the antioxidant activity of the wines correlated closely with the concentration of polyphenolic compounds and these parameters were significantly higher after contact with medium-toasted chips. The apple wines had high values of lightness and yellow color, and the addition of chips did not significantly affect the color parameters (CIELAB). In the sensory assessment, the control wine (without chips) received the lowest scores, while significantly higher scores were given to the wine with the addition of 6 g/L of heavily-toasted chips, which was characterized by intense smoky, toasty, woody and vanilla notes.
A study was conducted to investigate the effects of oak chips on the quality of persimmon brandy. The brandy was prepared from Mopan persimmons through fermentation and distillation, and aged for ...30–210 days with 0, 5, 10, and 15 g/L of oak chips. The brandy was analyzed for total phenols, oxidation resistance, color, volatile compounds, and non-volatile compounds. Results showed that the addition of oak chips increased the total phenolic content and DPPH scavenging capacity of the brandy. The brandy achieved a better golden yellow color when aged with 10 and 15 g/L of oak chips. HS-SPME-GC-MS analysis revealed 14, 22, 26, and 21 compounds in the four brandy samples with different amounts of oak chips. The brandy aged with 10 g/L of oak chips had the highest total content of volatile compounds. LC-MS-based metabolomics identified a total of 618 non-volatile metabolites, with 20 having the highest relative expression when aged with 10 g/L of oak chips. These findings suggest that persimmon brandy achieves better quality and flavor when aged with 10 g/L of oak chips for 210 days.
•Oak chips increased the persimmon brandy's phenolic content and achieved a golden yellow color.•Persimmon brandy aged with 10 g/L of oak chips had the highest total content of volatile compounds.•More than 600 non-volatile metabolites were identified in Persimmon brandy aged by oak chips.
The feasibility of accelerating the release of volatile compounds of oak wood chips and aged aroma in wines by ultrasounds and microwaves techniques has been assessed.
Despite the influence of the ...oak wood origin on the extraction of volatile compounds, results showed that wines subjected to treatments of ultrasounds 400 W during 12 h with pulses on/off each hour and microwaves 700 W for 20 min reached similar concentrations of compounds released from oak chips in wines macerated for 8 days. Those wines treated with microwaves exhibited more oak wood related compounds, but ultrasounds enhanced the extraction of more relevant compounds from a sensorial point of view. Consequently, wines with an accelerated ageing assisted by ultrasounds acquired more pronounced aged aromas. Therefore, the use of ultrasound to assist ageing process resulted in an accelerated acquisition of aged aroma which may resemble or even enhance the sensorial profile of wines in contact with oak chips in shorter times.
•Ultrasounds and microwaves techniques for accelerating aged wine process.•Extraction kinetics depend on the nature of oak wood compounds and wood origin.•Wines treated with microwaves exhibited more volatile oak wood compounds.•Ultrasounds favored the extraction of the most sensorially significant compounds.•Ultrasound treatment resembles better aging process in the shortest possible time.
•The addition of oak chips during red-wine fermentation has been evaluated.•That wood-grape mix maceration process increased the content in co-pigments.•Pigment content and colour effects depend on ...the maceration time and chip dose.•More stable colour in wines fermented with oak chips and shorter maceration time.•Long maceration with oak chips could favour lighter colour by pigment adsorption.
Oak chips-related phenolics are able to modify the composition of red wine and modulate the colour stability. In this study, the effect of two maceration techniques, traditional and oak chips-grape mix process, on the phenolic composition and colour of Syrah red wines from warm climate was studied. Two doses of oak chips (3 and 6g/L) at two maceration times (5 and 10days) during fermentation was considered. Changes on phenolic composition (HPLC–DAD–MS), copigmentation/polymerisation (spectrophotometry), and colour (Tristimulus and Differential Colorimetry) were assessed by multivariate statistical techniques. The addition of oak chips at shorter maceration times enhanced phenolic extraction, colour and its stabilisation in comparison to the traditional maceration. On contrast, increasing chip dose in extended maceration time resulted in wines with lighter and less stable colour. Results open the possibility of optimise alternative technological applications to traditional grape maceration for avoiding the common loss of colour of wines from warm climate.
•Controlled oxygen dose through MOX (in bulk or barrels) promotes vinegar quality.•MOX with oak chips mimics and efficiently accelerates the oak barrel aging process.•MOX induced higher concentration ...of phenolic compounds in shorter aging period.•MOX reduced the aging period to 1/3 compared to barrel aging.•Aromatic profile of 1.5-year barrel aged vinegar was similar to 6 months MOX aged.
The effect of micro-oxygenation (MOX) technique on quality and sensorial characteristics of balsamic vinegar was investigated, aiming to aging acceleration. Aging experiments were conducted using a multiple diffuser micro-oxygenator for up to 6 months with an oxygen flow of 30 mg/L/month, including oak chips (1 g/L) or not. Barrel maturation was simultaneously carried out. Quality, nutritional, sensorial characteristics and the aromatic profile of all aged vinegars were evaluated throughout aging. MOX accelerated the alteration of aging indices. Volatile compounds of fruity aroma and wine were decreased, while the fatty/buttery and caramel aroma compounds were increased. Similar compounds of 1.5-year barrel maturation were developed within 6 and 5 months applying MOX without or with oak chips, respectively. MOX resulted in reduction of the aging time to 1/3 compared to the corresponding one in barrels, considered as an attractive approach for vinegar-producing industries, mimicking and accelerating the long and costly barrel aging.
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•Adhesion properties of Candida zemplinina on abiotic surfaces were evaluated.•Strain dependent adhesion profile was observed.•Two different adhesion profiles were identified when C. ...zemplinina was adhered on stainless steel chips.•Candida zemplinina cells attached on oak chips influence wine characteristics.•Candida zemplinina cells attached on oak chips enhanced wine glycerol and esters content.
In this study cell surface hydrophobicity and the ability to adhere on abiotic surfaces (polystyrene plates, stainless steel and oak chips) of 10 Candida zemplinina strains were assessed. Moreover, the impact of C. zemplinina cells adhered on oak surface on fermentation kinetics and volatile profile of Montepulciano d’Abruzzo organic wines was evaluated. All strains showed a hydrophobic nature with a certain affinity for the apolar solvents tested (hexadecane and decane). In agreement with this data strains were able to adhere on abiotic surfaces in a strain dependent way. On polystyrene plates all strains mainly grew as planktonic cells. On stainless steel surfaces sessile cells ranged from 2.6 Log CFU/mL (SB2) to 4.1 Log CFU/mL (SB8), while on oak chips were about 2 log higher ranging from 4.3 Log CFU/mL (SB8) to 6.1 Log CFU/mL (SB10). Candida zemplinina sessile state resulted in an increase of glycerol (from 6.98 g/L to 11.92 g/L) and esters amount (from 55.47 g/L to 91.5 mg/L), and a reduction of ethanol content (from 14.13% to 9.12% v/v). As for esters, methyl vanillate, ethyl isobutyrate, and ethyl isovalerate were present only when C. zemplinina was adhered on oak chips. This study revealed that changes of concentrations in esters and glycerol content reflected the fermentation bioactivity of yeast cells attached on oak chips. Surface-adhered behaviours should be considered in the improvement of strategies for the development of high-quality organic wines and eventually obtain novel wine styles.
The effects of size, toasting degree, and time of contact on the release of volatile compounds from Quercus alba (L.) chips during a simulated fermentation and post-fermentative process were studied. ...The results obtained indicated that the large-size chips favored the release of furfural and furfuryl alcohol, while the small ones increased the concentration of cyclotene and maltol. The interaction between chip size and time of contact showed that the small-size chips are more sensitive to the increase of ethanol concentration for the extraction rate of some compounds (furfural, vanillin, maltol, cyclotene, whiskey lactones, and eugenol) compared to the large-size ones, increasing their concentrations at the end of maceration. The toasting degree of oak chips had a different influence on the volatile compounds studied. Cyclotene and guaiacol concentrations increased with the toasting intensity, whereas the extracted concentration of all compounds increased from light to medium-toasted chips, except for eugenol, and then decreased by further increasing the toasting level for 5-methylfurfural, whiskey lactones, eugenol, and only using high-level toasted chips for furfuryl alcohol, maltol, and vanillin. A possible protection effect of the chip size toward the possible degradation or volatilization losses of furfural for high toasting degrees was observed.
•A young red wine was processed by high pressure processing (HHP) with oak chips.•Phenolic content and antioxidant activity of wine increased after processing.•The property of HHP-oak treated wines ...was more affected by “pressure holding time”.•Sensory property of wine changed after oak chip maceration with and without HHP.
The influence of high hydrostatic pressure (HHP) processing in parallel with oak chip maceration on the physicochemical and sensory properties of a young red wine was investigated preliminarily. Wines were treated by HHP at 250, 450 and 650MPa for up to 45min and French oak chips (5g/L) were added. HHP enhanced the extraction of phenolics from oak chips. The phenolic contents and antioxidant activity of the wine increased after HHP processing in the presence of oak chips. Meanwhile, the anthocyanin content and wine color intensity decreased in the first 5min of pressure treatment and then increased gradually. The multivariate analysis revealed that “pressure holding time” was the key factor affecting wine physicochemical characteristics during HHP processing in the presence of oak chips. Furthermore, oak chip maceration with and without HHP processing weakened the intensities of several sensory attributes and provided the wine with an artificial taste.
•Quercus humboldtii could be a good alternative wood source for ageing wines.•Colombian chips and wines aged with them had lower furfural and (Z)-Whisky lactone concentrations.•5-Methylfurfural, ...guaiacol, isoeugenol, syringol contents were higher in Colombian samples.•Wines treated with Colombian oak showed higher smoky and lower coconut notes.
Different oak species or origins have been studied to find an alternative to traditional ones and Quercus humboldtii from Colombia is a candidate. Some studies analyse the composition of this oak, but no work has been found to study its use for wine treatment. The aim was to evaluate volatile composition of toasted Q. humboldtii oak chips and the wines treated with these chips. To evaluate its oenological potential Q. alba and Q. petraea have been included in this trial. The wines were subjected to a sensory analysis. Results indicated that oak chips and wines macerated for 90 days with toasted Colombian chips exhibited higher 5-methylfurfural, guaiacol, trans-isoeugenol and syringol concentrations than others, while the furfural and cis-β-methyl-γ-octalactone content was lower. Sensory analysis showed that the wines treated with Colombian oak presented more notes of smoked and less of coconut. Therefore, this oak could probably be considered suitable for ageing.
The extractability of the main oak ellagitannins has been studied in five model solutions containing different types of oak chips (two sizes and different toasting degrees for each size). A new ...extraction kinetic model has been proposed from the quantitative experimental results obtained by means of HPLC–ESI-MS/MS-multiple reaction monitoring method. The model considers an initial extraction (i.e., washing step) followed by a diffusion step, which involves two different processes that follow first-order kinetics at different rates. Differences in the extractability of the ellagitannins in the different model solutions have been observed and explained on the basis of the kinetic model here proposed.
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