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Ren, Yuan‐Yuan; Mao, Hong‐Xiang; Hu, Meng‐Yang; Zhu, Shou‐Fei; Zhou, Qi‐Lin
ChemCatChem, September 4, 2020, Letnik: 12, Številka: 17Journal Article
A carbene insertion into electron‐deficient C−H bonds of 1,3‐diesters, β‐ketoesters, β‐ketonitriles, and malononitriles was realized by using CuCN/PCy3 as the catalyst. The reaction provides a straightforward approach to the synthetically important multi‐substituted succinic acid derivatives. A plausible reaction mechanism with cyclopropanation/ring opening as key steps was proposed based on control experiments. Copper catalysis: A formal carbene insertion into electron‐deficient C−H bonds of 1,3‐diesters, β‐ketoesters, β‐ketonitriles, and malononitriles was realized by using CuCN/PCy3 as the catalyst. The reaction provides a straightforward approach to the multi‐substituted succinic acid derivatives. The mechanistic studies suggested that this formal C−H bond insertion reaction likely proceeds through a cyclopropanation of enol and a ring‐opening reaction sequence.
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JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
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in: SICRIS
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