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Abhyankar, Nandita; Bertaina, Sylvain; Orio, Maylis; Dalal, Naresh S.
Ferroelectrics, 10/2018, Letnik: 534, Številka: 1Journal Article
We employ electron paramagnetic resonance (EPR) of the spin probe Mn 2+ to study the paraelectric − ferroelectric transition in Dimethylammonium Manganese Formate (DMMnF) and Mn 2+ -doped Dimethylammonium Zinc Formate (DMZnF), which are considered model metal − organic frameworks (MOF) with a Pb-free perovskite architecture. In DMMnF, we study the variation of the Mn 2+ EPR line shape and intensity at the X-band (∼9.4 GHz) and over 80 to 300 K, and we show the absence of magnetoelectric coupling at the ferroelectric transition. At the antiferromagnetic transition in DMMnF, we detect a magnetoelectric coupling caused by weak ferromagnetism in the AFM phase. In DMZnF, EPR spectra of the Mn 2+ probe combined with DFT show that the crystal field is predominantly determined by the Dimethylammonium (DMA + ) cations.
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