One major challenge of implementing Directed Energy Deposition (DED) Additive Manufacturing (AM) for production is the lack of understanding of its underlying process-structure-property relationship. ...Parts manufactured using the DED technologies may be too inconsistent and unreliable to meet the stringent requirements for many industrial applications. The objective of this research is to characterize the underlying thermo-physical dynamics of the DED process, captured by melt pool signals, and predict porosity during the build. Herein we propose a novel porosity prediction method based on the temperature distribution of the top surface of the melt pool as an AM part is being built. Self-Organizing Maps (SOMs) are then used to further analyze the two-dimensional melt pool image streams to identify similar and dissimilar melt pools. X-ray tomography is used to experimentally locate porosity within the Ti-6Al-4V thin-wall specimen, which is then compared with predicted porosity locations based on the melt pool analysis. Results show that the proposed method based on the temperature distribution of the melt pool is able to predict the location of porosity almost 96% of the time when the appropriate SOM model using a thermal profile is selected. Results are also compared with a previous study, that focuses only on the shape and size of the melt pool. We find that the incorporation of thermal distribution significantly improves the accuracy of porosity prediction. The significance of the proposed methodology based on the melt pool profiles is that this can lead the way toward in situ monitoring and minimize or even eliminate pores within the AM parts.
A three dimensional finite element model (FEM) is introduced in this work in order to simulate the melt pool size during the Selective Laser Melting (SLM) process. The model adopts the Optical ...Penetration Depth (OPD) of laser beam into the powder bed and its dependency on the powder size in definition of the heat source. The model is used to simulate laser melting of a single layer of stainless steel 316L on a thick powder bed. The results of the model for the melt pool depth are validated with the experimental results. The model is then used to predict the effect of different scanning speeds on the melt pool depth, width, and length. The results showed that the melt pool size varies from the beginning of a track to its end and from the first track to the next. The melt pool size, however, reaches a stable condition after a few tracks. This concept was used to simplify the process modeling in which reduces the computational costs.
Display omitted
•The developed Finite Element model is able to predict the melt pool size accurately in the SLM process.•The rate of change in the width of the melt pool by altering the speed is not the same as that of the depth.•The melt pool dimensions reached a steady condition after the third track.•The melt pool depth of each track stayed almost constant after about 2mm from the beginning of the track.
The high‐speed synchrotron X‐ray imaging technique was synchronized with a custom‐built laser‐melting setup to capture the dynamics of laser powder‐bed fusion processes in situ. Various significant ...phenomena, including vapor‐depression and melt‐pool dynamics and powder‐spatter ejection, were captured with high spatial and temporal resolution. Imaging frame rates of up to 10 MHz were used to capture the rapid changes in these highly dynamic phenomena. At the same time, relatively slow frame rates were employed to capture large‐scale changes during the process. This experimental platform will be vital in the further understanding of laser additive manufacturing processes and will be particularly helpful in guiding efforts to reduce or eliminate microstructural defects in additively manufactured parts.
The high‐speed synchrotron X‐ray imaging technique was synchronized with a custom‐built laser‐melting setup to capture the dynamics of laser powder‐bed fusion processes in situ. Various significant phenomena, including vapor‐depression and melt‐pool dynamics and powder‐spatter ejection, were captured with high spatial and temporal resolution.
In-depth understanding of microstructure development is required to fabricate high quality products by additive manufacturing (for example, 3D printing). Here we report the governing role of ...side-branching in the microstructure development of alloys by laser powder bed fusion. We show that perturbations on the sides of cells (or dendrites) facilitate crystals to change growth direction by side-branching along orthogonal directions in response to changes in local heat flux. While the continuous epitaxial growth is responsible for slender columnar grains confined to the centreline of melt pools, side-branching frequently happening on the sides of melt pools enables crystals to follow drastic changes in thermal gradient across adjacent melt pools, resulting in substantial broadening of grains. The variation of scan pattern can interrupt the vertical columnar microstructure, but promotes both in-layer and out-of-layer side-branching, in particular resulting in the helical growth of microstructure in a chessboard strategy with 67° rotation between layers.
Display omitted
•A novel calibration method is proposed to calculate the absorption coefficient.•The numerical method is able to predict the melt pool shape on a wide process window.•The transition ...from low keyhole melt pool morphology to deep keyhole is correctly described.•Metal ejections during laser-matter interaction need to be considered in the simulation.
Numerical simulation is a powerful tool to understand the link between processing parameters and solidification conditions during the laser beam melting (LBM) process. To be able to use this tool for microstructural control, numerical models need to be validated on a large set of experimental conditions, to ensure that the model describes the predominant physical phenomena. In this study, an experimental set of twenty tracks was produced in an Inconel 738 alloy, with a wide range of energy input and scanning speed. Experimental melt pool shapes were compared to the predictions of a multiphysics numerical model. In this model, the powder bed is considered as a continuum. The laser source is modeled with a Beer-Lambert absorption law, and surface tension, Marangoni force and recoil pressure are the driving forces for melt pool dynamics. This kind of model offers an efficient computational time, but requires a calibration of the absorption coefficient and a representative description of laser-matter interaction. In order to represent correctly heat and mass transfer during laser-matter interaction, the model needs to account for the loss of matter caused by the ejection of powder particles and spatters. A novel calibration method was proposed to calculate the absorption coefficient. This method uses the experimental cross sections of the melt pools and a simplified analytical expression of energy balance. The use of this calibration method enabled a good agreement between experiments and calculations on a large process window. The values obtained by the calibrations resulted in a phenomenological expression of absorptivity coefficient with process parameters. Based on this expression, a comparison was made with another numerical model from literature using a time-consuming ray-tracing method in order to calculate the absorptivity coefficient. Similar results have been obtained, demonstrating the potential of the proposed approach to predict the melt pool shape and thus better understand the combined effect of laser-matter interaction and solidification in LBM process.
Selective laser melting (SLM) is a relatively new manufacturing technique that can be used to process a range of materials. Aluminum alloys are potential candidates for SLM but are more difficult to ...process than the titanium alloys more commonly used with this technique. This is because of the former’s physical properties that can result in high levels of porosity in the final parts. Although the majority of studies to date into the processing of Al alloys by SLM have considered the development of load bearing objects, in particular porosity reduction and mechanical characterization of the parts, it is also important to study the single tracks formed during the process. This paper studies the effect of changing the scan speed on the formation of fusion lines and single tracks from an Al alloy, as well as their overlap to form a single layer. The geometrical features of the melt pools as well as the boundaries of continuity and/or irregularities were defined and showed dependence on scan speed. Keyhole mode melting domination was observed. The scan tracks and layers were porosity-free suggesting pores to form with layer accumulation. Investigations showed that increasing the layer thickness should be avoided as it promoted defects. Energy dispersive X-ray (EDX) mapping was implemented to compare the chemical composition distribution in the SLM material and its as-cast counterpart. A fine microstructure with homogenous distribution of the alloying elements was observed. Nanoindentation and EDX were used to establish an understanding of the hardness profile across melt pools of single tracks and their interrelation to the chemical composition. The elemental distribution yielded uniform high nano-hardness with no spatial variation across the SLM material.
Understanding laser interaction with metal powder beds is critical in predicting optimum processing regimes in laser powder bed fusion additive manufacturing of metals. In this work, we study the ...denudation of metal powders that is observed near the laser scan path as a function of laser parameters and ambient gas pressure. We show that the observed depletion of metal powder particles in the zone immediately surrounding the solidified track is due to a competition between outward metal vapor flux directed away from the laser spot and entrainment of powder particles in a shear flow of gas driven by a metal vapor jet at the melt track. Between atmospheric pressure and ∼10 Torr of Ar gas, the denuded zone width increases with decreasing ambient gas pressure and is dominated by entrainment from inward gas flow. The denuded zone then decreases from 10 to 2.2 Torr reaching a minimum before increasing again from 2.2 to 0.5 Torr where metal vapor flux and expansion from the melt pool dominates. The dynamics of the denudation process were captured using high-speed imaging, revealing that the particle movement is a complex interplay among melt pool geometry, metal vapor flow, and ambient gas pressure. The experimental results are rationalized through finite element simulations of the melt track formation and resulting vapor flow patterns. The results presented here represent new insights to denudation and melt track formation that can be important for the prediction and minimization of void defects and surface roughness in additively manufactured metal components.
Display omitted
In the present study, we examined changes in the microstructure and mechanical properties of AlSi10Mg alloy, initially fabricated using selective laser melting (SLM) combined with a powder-bed ...system, by applying heat treatments at temperatures of either 300 or 530°C. The as-fabricated samples exhibited a characteristic microstructural morphology and {001} texture. Melt pools corresponding to the locally melted and rapidly solidified regions were found to be composed of several columnar α-Al grains surrounded by fine eutectic Si particles. A fine dislocation substructure consisting of low-angle boundaries is present within the columnar α-Al grains. At elevated temperatures, fine Si phase precipitates within the columnar α-Al phase and coarsening of the eutectic Si particles occurs. These fine Si particles inhibit grain growth in the α-Al matrix, resulting in the microstructural morphology and 001 texture observed in the heat-treated samples. The dislocation substructure disappears in the columnar α-Al grains. Furthermore, the formation of a stable intermetallic phase occurs, reaching microstructural equilibrium after long-term exposure. The as-fabricated specimen exhibits a high tensile strength of approximately 480MPa. The strength is independent of the tensile direction, that is, normal and parallel to the building direction. In contrast, the tensile ductility is found to be direction-dependent, and is therefore responsible for a fracture preferentially occurring at a melt pool boundary. The direction-dependence of the tensile ductility was not found in the specimen that had been heat-treated at 530°C. The present results provide new insights into the control of the direction-dependence of the tensile properties of AlSi10Mg alloys fabricated by SLM.
Display omitted
In this study, 316L parts were fabricated with the selective laser melting additive layer manufacturing process using unidirectional laser scan to control their texture. The melt pool ...shape, microstructure and texture of three different cubic samples were analyzed and quantified using optical microscopy and electron back-scattered diffraction. The samples scanned along the shielding gas flow direction were shown to exhibit shallow conduction melt pools together with a strong {110} Goss texture along the laser scanning direction. The sample prepared with a laser scan perpendicular to the gas flow direction had deeper melt pools, with a weaker {110} Goss texture in addition to a fiber texture parallel to the scanning direction. Correlations were proposed between the melt-pool geometry and overlap and the resulting texture. The decrease of the melt pool depth was assumed to be linked to local attenuation of the laser beam effective power density transmitted to the powder bed.
Overhanging and floating layers which are introduced during the build in selective laser melting (SLM) process are usually associated with high temperature gradients and thermal stresses. As there is ...no underlying solid material, less heat is dissipated to the powder bed and the melted layer is free to deform resulting undesired effects such as shrinkage and crack. This study uses three-dimensional finite element simulation to investigate the temperature and stress fields in single 316L stainless steel layers built on the powder bed without support in SLM. A non-linear transient model based on sequentially coupled thermo-mechanical field analysis code was developed in ANSYS parametric design language (APDL). It is found that the predicted length of the melt pool increases at higher scan speed while both width and depth of the melt pool decreases. The cyclic melting and cooling rates in the scanned tracks result high VonMises stresses in the consolidated tracks of the layer.