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  • Melting point of dried gold nanoparticles prepared with ultrasonic spray pyrolysis and lyophilisation [Elektronski vir]
    Jelen, Žiga, 1993- ...
    A coupled process of ultrasonic spray pyrolysis and lyophilisation was used for the synthesis of dried gold nanoparticles. Two methods were applied for determining their melting temperature: uniaxial ... microcompression and differential scanning calorimetry (DSC) analysis. Uniaxial microcompression resulted in sintering of the dried gold nanoparticles at room temperature with an activation energy of 26–32.5 J/g, which made it impossible to evaluate their melting point. Using DSC, the melting point of the dried gold nanoparticles was measured to be around 1064.3°C, which is close to pure gold. The reason for the absence of a melting point depression in dried gold nanoparticles was their exothermic sintering between 712 and 908.1°C.
    Source: Nanotechnology reviews : Elektronski vir. - ISSN 2191-9097 (Vol. 12, iss. 1, July 2023, 12 str.)
    Type of material - e-article ; adult, serious
    Publish date - 2023
    Language - english
    COBISS.SI-ID - 158645507

    Link(s):

    Digital Library of the University of Maribor – DLUM
    DOI

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