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Sinteza bakrovih, kobaltovih in nikljevih koordinacijskih spojin z izoniazidom = Synthesis of copper, cobalt and nickel coordiantion compounds with isoniazid : diplomsko deloHrastar, SabinaV diplomskem delu sem se ukvarjala s sintezo in karakterizacijo novih bakrovih, kobaltovih in nikljevih koordinacijskih spojin. Za sintezo smo uporabili bakrov acetat monohidrat, kobaltov acetat ... tetrahidrat in nikljev acetata tetrahidrat ter ligand izoniazid. Izvedli smo sedemdeset sinteznih reakcij, pri čemer smo spreminjali različne parametre: čas sinteze, temperaturo, topilo (destilirana voda, metanol, etanol, aceton, acetonitril, tetrahidrofuran, diklorometan, N,N-dimetilformamid) in postopek sinteze (sobna temperatura, sinteza na refluksu in solvotermalna sinteza). Topilo smo izbrali glede na predhodno opravljen preizkus topnosti reagentov v posameznem topilu. Sintetizirane spojine smo karakterizirali z rentgensko praškovno difrakcijo, termogravimetrično analizo, Fourierjevo transformacijsko infrardečo spektroskopijo in rentgensko strukturno analizo na monokristalu. Rezultati analiz so pokazali na nastanek štirih različni bakrovih, treh različnih kobaltovih in treh različnih nikljevih produktov. Za rentgensko strukturno analizo na monokristalu sta bila primerna bakrov in kobaltov produkt. Gre za kompleksa [Cu(INA)2(H2O)4] in [Co(INA)2(H2O)4], ki sta že znana.Type of material - undergraduate thesis ; adult, seriousPublication and manufacture - Maribor : [S. Hrastar], 2016Language - slovenianCOBISS.SI-ID - 22188040
Author
Hrastar, Sabina
Other authors
Kristl, Matjaž |
Dojer, Brina
Topics
Univerzitetna in visokošolska dela |
diplomska dela |
koordinacijske spojine |
baker |
kobalt |
nikelj |
izoniazid |
rentgenska praškovna difrakcija (p-XRD) |
termogravimetrična analiza (TGA) |
Fourierjeva transformacijska infrardeča spektroskopija (FTIR) |
rentgenska strukturna analiza na monokristalu |
theses |
coordination compounds |
copper |
cobalt |
nickel |
isoniazid |
powder X-ray diffraction (p-XRD) |
thermogravimetric analysis (TGA) |
Fourier transform infrared spectroscopy (FTIR) |
single-crystal X-ray diffraction
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Library | Call number – location, accession no. ... | Copy status |
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Miklošič Library FPNM, Maribor | M DIPL 54 HRASTAR S. Sinteza IN: 920160022 |
available - reading room |
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Database name | Field | Year |
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Hrastar, Sabina | ![]() |
Kristl, Matjaž | 14755 |
Dojer, Brina | 29578 |
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