Sinteza in karakterizacija nikljevih koordinacijskih spojin z izbranimi tiopiridinskimi ligandi; Synthesis and characterization of coordination compounds with nickel using thiopyridine ligands : magistrsko delo

(UM)

Sinteza in karakterizacija nikljevih koordinacijskih spojin z izbranimi tiopiridinskimi ligandi = Synthesis and characterization of coordination compounds with nickel using thiopyridine ligands : magistrsko delo

Breznik, Katja, 1992-

Namen magistrskega dela je bila sinteza novih koordinacijskih spojin z nikljem. Pri tem je bil uporabljen nikljev acetat tetrahidrat in različni tiopiridinski ligandi. Opravljenih je bilo 36 sintez. ... Sinteze so bile v največji meri izvedene z mešanjem pri sobni temperaturi, v določenih primerih pa z refluktiranjem in solvotermalno pri povišani temperaturi in tlaku. Kot topili sta bila v večini primerov uporabljena metanol in N,N-dimetilformamid. Pogosto smo uporabili tudi ustrezno kombinacijo topil. Dobljeni sintezni produkti so bili karakterizirani z infrardečo spektroskopijo, rentgensko analizo na monokristalu in rentgensko praškovno difrakcijo. Dodatne informacije o strukturi in lastnostih spojin smo pridobili z magnetnimi meritvami in s termogravimetrično analizo. V okviru magistrskega dela je bila uspešno sintetizirana do sedaj še neznana koordinacijska spojina s kemijsko formulo: [Ni(O2CCH3)2(C7H6N2S)2]. Gre za enojedrno koordinacijsko spojino z nikljem, na katerega sta vezana dva enovezna liganda, molekuli 2-aminobenzotiazola in dva kelatno vezana acetatna liganda. Sinteza je bila izvedena z mešanjem pri sobni temperaturi, na zraku. Kot topilo je bil uporabljen metanol.

Type of material - master's thesis ; adult, serious

Publication and manufacture - Maribor : [K. Breznik], 2017

Language - slovenian

COBISS.SI-ID - 23161352

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Digital Library of the University of Maribor – DLUM

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Author
Breznik, Katja, 1992-

Other authors
Kristl, Matjaž | Dojer, Brina

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Library	Call number – location, accession no. ...	Copy status
Miklošič Library FPNM, Maribor	D MAG 54 BREZNIK K. Sinteza IN: 920170015	available - reading room

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Year	Impact factor		Edition		Category		Classification
Year	JCR	SNIP	JCR	SNIP	JCR	SNIP	JCR	SNIP

Links to authors' personal bibliographies	Links to information on researchers in the SICRIS system
Breznik, Katja, 1992-
Kristl, Matjaž	14755
Dojer, Brina	29578

Source: Personal bibliographies and: SICRIS

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