Validacija analiznih metod rastlinskih zaščitnih sredstev z uporabo tekočinske kromatografije : poročilo o rezultatih opravljenega dela na raziskovalnem projektu v letu 1996/1997 [za RSM Maribor]
Brodnjak-Vončina, Darinka
Raziskovalna naloga obsega validacijo analiznega postopka izotiazolonov. Novi predpisi o izvajanju analiz v skladu z zahtevami ISO 900 in EN 45001 nas obvezujejo, da izvajamo analizne metode po ...kriterijih o zagotovitvi kvalitete dela (QA) in dobre laboratorijske prakse (Good Laboratiry Practice). Najprej smo izvedli predhodno validacijo analiznega postopka, ki zajema izbiro analizne metode za določen vzorec in optimizacijo metode (izbira sestave topil, mobilne faze, izbira kolone, temperature kolone, pritiska, itd.) Po optimizaciji smo izvedli kompletno validacijo. Kompletna validacija zajema pripravo vzorcev, pripravo standardnih raztopin za umiritveno krivuljo, pripravo vzorčnih raztopin ter primerjavo rezultatov, dobljenih z umiritveno krivuljo merjene komponente same ter umeritvene krivulje vzorčnih raztopin z merjeno komponento ter statistično vrednoenje dobljenih rezultatov. logo smo izvedli navzorčnem modelu analize izotiazolonov v vzorcih PBK in PBK 1.5.
Type of material - research report
Publication and manufacture - Maribor : Fakulteta za kemijo in kemijsko tehnologijo, 1997
pisarna A-003 (FS) RN-FKKT-97 BRODNJAK V. VALIDACIJA
available - reading room
University of Maribor Library
Skladišče II 95602
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