Divergent Titanium-Mediated Allylations with Modulation by Nickel or Palladium

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Divergent Titanium-Mediated Allylations with Modulation by Nickel or Palladium

Campaña, Araceli G; Bazdi, Btissam; Fuentes, Noelia; Robles, Rafael; Cuerva, Juan M; Oltra, J. Enrique; Porcel, Susana; Echavarren, Antonio M

Angewandte Chemie, September 15, 2008, Volume: 47, Issue: 39

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Palladium and nickel are used in conjunction with titanocene(III) complexes to perform selective allylations of carbonyl compounds and alkenes, respectively. Pd/Ti‐catalyzed allylation of ketones proceeds diastereoselectively under mild conditions, whereas Ni/Ti‐promoted cyclizations provide polyalkyl‐substituted carbo‐ and heterocycles with excellent control over regio‐ and stereoselectivity.

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