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Allu, Srinivasarao; Kumara Swamy, K. C.
Advanced synthesis & catalysis, August 24, 2015, Volume: 357, Issue: 12Journal Article
Indole‐substituted purine nucleobases have been synthesized by Ru‐catalyzed oxidative annulation of 6‐anilinopurines with internal alkynes that involves CH activation. Unsymmetrical aryl(alkyl)alkynes led to high regioselectivity. The reaction was also successful with nucleosides by delivering unprotected indole‐substituted nucleosides. In the presence of RuCl2(p‐cymene)2 and copper(II) acetate hydrate Cu(OAc)2⋅H2O, in some cases, we have observed two‐fold CH activation products that exhibit fluorescence. A ruthenacycle intermediate was characterized by crystallography, which suggests that the N‐1 nitrogen atom of the purine acts as a directing group for the present transformation.
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