Mechanochemical Dimerization of Aldoximes to Furoxans

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Mechanochemical Dimerization of Aldoximes to Furoxans

Fang, Run-Kai; Chen, Kuan; Niu, Chuang; Wang, Guan-Wu

Molecules (Basel, Switzerland), 04/2022, Volume: 27, Issue: 8

Journal Article

Solvent-free mechanical milling is a new, environmentally friendly and cost-effective technology that is now widely used in the field of organic synthesis. The mechanochemical solvent-free synthesis of furoxans from aldoximes was achieved through dimerization of the in situ generated nitrile oxides in the presence of sodium chloride, Oxone and a base. A variety of furoxans was obtained with up to a 92% yield. The present protocol has the advantages of high reaction efficiency and mild reaction conditions.

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Fang, Run-Kai | Chen, Kuan | Niu, Chuang | Wang, Guan-Wu

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