Lewis Acid Promoted Stereoselective Synthesis of Polysubstituted 1,3‐Dienes via a Dual 1,3‐Sulfur Rearrangement

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Lewis Acid Promoted Stereoselective Synthesis of Polysubstituted 1,3‐Dienes via a Dual 1,3‐Sulfur Rearrangement

Li, Rui‐Peng; Li, Jia; Chen, Xi; Liu, Jian; Wang, Xiaolei; Tang, Shouchu

Advanced synthesis & catalysis, December 20, 2022, Volume: 364, Issue: 24

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1,3‐Dienes are prevalent substructures in biologically active molecules and versatile building blocks in synthetic chemistry. Herein, using Lewis acids promoted dual 1,3‐sulfur rearrangements, we developed an approach for the direct synthesis of 1,3‐dithianyl substituted dienes. This method enabled the synthesis of tri‐ and tetra‐substituted 1,3‐dienes with high stereoselectivity and good yield under mild reaction conditions.

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