Crystallographic texturing of polycrystalline ferroelectric ceramics offers a means of achieving significant enhancements in the piezoelectric response. Templated grain growth (TGG) enables the ...fabrication of textured ceramics with single crystal-like properties, as well as single crystals. In TGG, nucleation and growth of the desired crystal on aligned single crystal template particles results in an increased fraction of oriented material with heating. To facilitate alignment during forming, template particles must be anisometric in shape. To serve as the preferred sites for epitaxy and subsequent oriented growth of the matrix, the template particles need to be single crystal and chemically stable up to the growth temperature. Besides templating the growth process, the template particles may also serve as seed sites for phase formation of a reactive matrix. This process, referred to as Reactive TGG (RTGG), has been used to obtain highly oriented Pb(Mg
1/3
Nb
2/3
)O
3
-PbTiO
3
, Sr
0.53
Ba
0.47
Nb
2
O
6
, and (Na
1/2
Bi
1/2
)TiO
3
-BaTiO
3
. Highly oriented Bi
4
Ti
3
O
12
, Sr
2
Nb
2
O
7
, CaBi
4
Ti
4
O
15
, Pb(Mg
1/3
Nb
2/3
)O
3
-PbTiO
3
, Sr
0.53
Ba
0.47
Nb
2
O
6
and (Na
1/2
Bi
1/2
)TiO
3
-BaTiO
3
ceramics have been produced by TGG. The resulting ceramics show texture levels up to 90%, and significant enhancements in the piezoelectric properties relative to randomly oriented ceramics with comparable densities. For example, piezoelectric coefficients of textured piezoelectrics are from 2 to 3 times higher than polycrystalline ceramics and as high as 90% of the single crystal values. In textured PMN-PT, a low field (< 5 kV/cm) piezoelectric coefficient (d
33
) of ∼1600 pC/N was obtained with > 0.3% strain (at 50 kV/cm). The high field dielectric and electromechanical properties of textured perovskites are more hysteretic than those of single crystals, probably as a result of clamping by the residual template particles, residual random grains, the presence of non-ferroelectric second phases, and a wide orientation distribution. Lateral clamping of one grain by another may also be an important factor in fiber-textured samples. Means to further improve the quality of texture and thus properties of textured piezoelectric ceramics by TGG are presented.
The KArlsruhe TRItium Neutrino (KATRIN) experiment will measure the absolute mass scale of neutrinos with a sensitivity of mν = 200 meV c2 by high-precision spectroscopy close to the tritium β-decay ...endpoint at 18.6 keV. Its Windowless Gaseous Tritium Source (WGTS) is a β-decay source of high intensity (1011 s−1) and stability, where high-purity molecular tritium at 30 K is circulated in a closed loop with a yearly throughput of 10 kg. To limit systematic effects the column density of the source has to be stabilized at the 10−3 level. This requires extensive sensor instrumentation and dedicated control and monitoring systems for parameters such as the beam tube temperature, injection pressure, gas composition and so on. In this paper, we give an overview of these systems including a dedicated laser-Raman system as well as several β-decay activity monitors. We also report on the results of the WGTS demonstrator and other large-scale test experiments giving proof-of-principle that all parameters relevant to the systematics can be controlled and monitored on the 10−3 level or better. As a result of these works, the WGTS systematics can be controlled within stringent margins, enabling the KATRIN experiment to explore the neutrino mass scale with the design sensitivity.
The aim of the KArlsruhe TRItium Neutrino experiment KATRIN is the determination of the absolute neutrino mass scale down to 0.2 eV, with essentially smaller model dependence than from cosmology and ...neutrinoless double beta decay. For this purpose, the integral electron energy spectrum is measured close to the endpoint of molecular tritium beta decay. The endpoint, together with the neutrino mass, should be fitted from the KATRIN data as a free parameter. The right-handed couplings change the electron energy spectrum close to the endpoint, therefore they have some effect also to the precise neutrino mass determination. The statistical calculations show that, using the endpoint as a free parameter, the unaccounted right-handed couplings constrained by many beta decay experiments can change the fitted neutrino mass value, relative to the true neutrino mass, by not larger than about 5–10%. Using, incorrectly, the endpoint as a fixed input parameter, the above change of the neutrino mass can be much larger, order of 100%, and for some cases it can happen that for large true neutrino mass value the fitted neutrino mass squared is negative. Publications using fixed endpoint and presenting large right-handed coupling effects to the neutrino mass determination are not relevant for the KATRIN experiment.
High Impedance TES Bolometers for EDELWEISS Marnieros, S.; Armengaud, E.; Arnaud, Q. ...
Journal of low temperature physics,
06/2023, Letnik:
211, Številka:
5-6
Journal Article
Recenzirano
The EDELWEISS collaboration aims for direct detection of light dark matter using germanium cryogenic detectors with low threshold phonon sensor technologies and efficient charge readout designs. We ...describe here the development of Ge bolometers equipped with high impedance thermistors based on a Nb
x
Si
1−x
TES alloy. High aspect ratio spiral designs allow the TES impedance to match with JFET or HEMT front-end amplifiers. We detail the behavior of the superconducting transition properties of these sensors and the detector optimization in terms of sensitivity to a-thermal phonons. We report preliminary results of a 200 g Ge detector that was calibrated using
71
Ge activation by neutrons at the LSM underground laboratory.
Abstract Conceptus estrogens and prostaglandins have long been considered the primary signals for maternal recognition of pregnancy (MRP) in the pig. However, loss-of-function studies targeting ...conceptus aromatase genes (CYP19A1 and CYP19A2) and prostaglandin–endoperoxide synthase 2 (PTGS2) indicated that conceptuses can not only signal MRP without estrogens or prostaglandins but can maintain early pregnancy. However, complete loss of estrogen production leads to abortion after day 25 of gestation. Although neither conceptus estrogens nor prostaglandins had a significant effect on early maintenance of corpora lutea (CL) function alone, the two conceptus factors have a biological relationship. To investigate the role that both conceptus estrogens and prostaglandins have on MRP and maintenance of pregnancy, a triple loss-of function model (TKO) was generated for conceptus CYP19A1, CYP19A2, and PTGS2. In addition, a conceptus CYP19A2−/− model (A2KO) was established to determine the role of placental estrogen during later pregnancy. Estrogen and prostaglandin synthesis were greatly reduced in TKO concept uses which resulted in a failure to inhibit luteolysis after day 15 of pregnancy despite the presence of conceptuses in the uterine lumen. However, A2KO placentae not only maintained functional CL but were able to maintain pregnancy to day 32 of gestation. Despite the loss of placental CYP19A2 expression, the allantois fluid content of estrogen was not affected as the placenta compensated by expressing CYP19A1 and CYP19A3, which are normally absent in controls. Results suggest conceptuses can signal MRP through production of conceptus PGE or stimulating PGE synthesis from the endometrium through conceptus estrogen. Failure of conceptuses to produce both factors results in failure of MRP and loss of pregnancy.