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Hou, Zhenshan; Theyssen, Nils; Brinkmann, Axel; Klementiev, Konstantin V.; Grünert, Wolfgang; Bühl, Michael; Schmidt, Wolfgang; Spliethoff, Bernd; Tesche, Bernd; Weidenthaler, Claudia; Leitner, Walter
Journal of catalysis, 09/2008, Letnik: 258, Številka: 2Journal Article
The preparation, characterization, and catalytic properties of Pd nanoparticles supported on mesoporous organic–inorganic hybrid materials are described for continuous-flow aerobic oxidation of alcohols using supercritical carbon dioxide (scCO 2) as a mobile phase. The nanoparticles were generated “bottom-up” from molecular precursors that were precoordinated to the support through suitable anchor units. The most active material allows high single-pass conversions in scCO 2 at temperatures as low as 60 °C. This high activity may be associated with the presence of small primary crystallites (approx. 2 nm) that conglomerate to ensembles about 25 nm in size, leading to a larger number of high-indexed planes in small volume units. These findings may provide useful guidelines for further catalyst design on the nanoscale for green oxidation methods.
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JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
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in: SICRIS
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